CLL736
| CLL736 | |
|---|---|
| Experimental Characterization of Multiphase Reactors | |
| Credits | 3 |
| Structure | 3-0-0 |
| Pre-requisites | CLL122, CLL222 |
| Overlaps | |
CLL736 : Experimental Characterization of Multiphase Reactors
[edit]Analytical techniques: Introduction to various analytical techniques e.g. GC, HPLC, UV Spectroscopy, TGA /DTA, FTIR, MS, GCMS, NMR, TOC, CHONS. Principle of measurement techniques, instruments and procedures. Calibration, data processing, analysis and interpretation. Few working demonstrations. Catalysis characterization: Introduction to various catalysis preparations and characterization techniques, e.g. porosity, surface area, pore volume and pore size distribution (using BET), XRD, SEM, TEM, NMR, AFM, ESCA. Mossabauer spectroscopy, chemisorption, TPD / TPR. Flow characterization: Introduction to single/multiphase flows/ reactors, role of hydrodynamics. Process parameters of interest, length and time scales, instantaneous vs. time averaged characteristics. Introduction to various advanced intrusive and non-intrusive flow measurement technqiues, e.g. mininaturized pressure probes, gamma-ray tomography, densitometry, PIV, RPT, ECT/ERT, high speed photography, tracers and radiotracers. Courses of Study 2024-2025 Chemical Engineering 131